含氟杀虫剂类农药的残留检测分析研究进展

doi:10.11924/j.issn.1000-6850.casb15010219

中国农学通报 ›› 2016, Vol. 32 ›› Issue (2): 68-72.doi: 10.11924/j.issn.1000-6850.casb15010219

所属专题：植物保护

含氟杀虫剂类农药的残留检测分析研究进展

王建芬¹,丁双阳²,王晓琳³

(¹北京市延庆县畜牧技术推广站,北京 102100；²中国农业大学动物医学院,北京 100129；³河南牧业经济学院,郑州 450046）

收稿日期:2015-01-28 修回日期:2015-11-30 接受日期:2015-12-03 出版日期:2016-01-28 发布日期:2016-01-28
通讯作者: 王晓琳
基金资助:
农业部公益性行业（农业）科研专项经费项目“食品质量安全‘主动’控制技术”(201203069-2)；奶牛产业技术体系北京市创新团队项目。

Research Progress of Analytical and Detection Methods of Fluorine-containing Pesticides Residues

Wang Jianfen¹, Ding Shuangyang², Wang Xiaolin³

(¹Beijing Yanqing Animal Husbandry Technology Extension Station, Beijing 102100;²College of Veterinary Medicine, China Agricultural University, Beijing 100129;³Henan University of Animal Husbandry and Economy, Zhengzhou 450046)

Received:2015-01-28 Revised:2015-11-30 Accepted:2015-12-03 Online:2016-01-28 Published:2016-01-28

摘要/Abstract

摘要： 由于氟原子所具有的特殊功效，近几十年来含氟类农药发展迅速。含氟杀虫剂主要包括拟除虫菊酯和苯甲酰脲中的含氟品种，以及氟虫腈、溴虫腈、茚虫威等杂环类化合物。本研究对含氟杀虫剂类农药的残留分析方法进行了综述，包括样品提取技术、净化技术及检测技术。样品净化技术包括固相萃取和液-液萃取，检测技术主要有气象色谱法、高效液相色谱法、气相色谱-质谱联用(GC-MS)和高效液相色谱-质谱联用(HPLC-MS)。最后从动物性食品安全的角度提出建议。

关键词: 农用地, 农用地, 质量等别, 空间技术, 经济耦合性, Moran散点图

Abstract: Because of the special function of fluorine atom for organism, fluorine-containing pesticide has been developed quickly in recent decades. The major classes of fluorine-containing pesticides are pyrethroid, benzoylurea and heterocyclic compounds which include fipronil, chlorfenapyr, indoxacarb, etc. In this study, the development of residue analytical methods including extraction, purification and detection techniques of fluorine-containing pesticide was described in detail. The purification techniques included solid-phase extraction and liquid-liquid extraction, the detection techniques included gas chromatography (GC), high performance liquid chromatography (HPLC), GC-MS and HPLC-MS. Finally suggestions were put forward from the aspect of animal derived food safety.

王建芬,丁双阳,王晓琳. 含氟杀虫剂类农药的残留检测分析研究进展[J]. 中国农学通报, 2016, 32(2): 68-72.

Wang Jianfen,Ding Shuangyang and Wang Xiaolin. Research Progress of Analytical and Detection Methods of Fluorine-containing Pesticides Residues[J]. Chinese Agricultural Science Bulletin, 2016, 32(2): 68-72.

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含氟杀虫剂类农药的残留检测分析研究进展

Research Progress of Analytical and Detection Methods of Fluorine-containing Pesticides Residues

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