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中国农学通报

中国农学通报 ›› 2009, Vol. 25 ›› Issue (23): 118-121.

• 食品 营养 检测 安全 • 上一篇    下一篇

微波消解ICP-MS法测定笋制品中的多种元素

陈惠云   

  • 收稿日期:2009-07-02 修回日期:2009-07-22 出版日期:2009-12-05 发布日期:2009-12-05
  • 基金资助:
    宁波市科学技术局农业科研攻关项目

Determination of Elements in Bamboo Shoot by ICP-MS with Microwave Digestion

  • Received:2009-07-02 Revised:2009-07-22 Online:2009-12-05 Published:2009-12-05

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摘要： 本研究采用微波消解样品、电感耦合等离子体质谱仪（ICP-MS）法同时测定笋制品中Ca、K、Mg、Al、Fe、Mn、Cu、As、Cd、Pb、Cr、Se 等12种元素。结果表明，添加回收率在86%~113%之间，相对标准偏差RSD<5%（n=6），检出限为0.002μg/L ~2.471μg/L。4种笋制品的元素含量具有一定的差异，主要是由于笋制品的配方不同所至。该法快速简便、准确率高、精密度好，可以用于笋制品中元素的测定。

关键词: 大叶黄杨, 大叶黄杨, 扦插生根, 植物生长调节剂

Abstract: In this study, 12 kind of elements etc. Ca, K, Mg, Al, Fe, Mn, Cu, As, Cd, Pb, Cr, Se in bamboo shoot products were determined by ICP-MS with microwave digestion. The results showed, the average recoveries were between 86% and 113%, the RSD<5%（n=6）, the limit of determination was 0.002μg/L ~2.471μg/L. The element contents of 4 bamboo shoot products were different, due to different material contents. The method is fast, simple and accurate, could be used to determine element contents in bamboo shoot products.