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中国农学通报 ›› 2025, Vol. 41 ›› Issue (2): 133-139.doi: 10.11924/j.issn.1000-6850.casb2024-0409

• 食品·营养·检测·安全 • 上一篇    下一篇

果蔬中农药残留检测前处理方法应用进展

欧帅(), 马诚仁, 王婧媛, 田秀秀, 高猛, 郭昕   

  1. 梁山县检验检测中心,山东济宁 272600
  • 收稿日期:2024-06-25 修回日期:2024-10-14 出版日期:2025-01-13 发布日期:2025-01-13
  • 作者简介:

    欧帅,男,1992年出生,工程师,硕士,主要从事农产品质量检验检测方面的工作。通信地址:272600 山东省济宁市梁山县拳铺镇泰福路16号 梁山县检验检测中心,Tel:0537-7690081,E-mail:

  • 基金资助:
    济宁市重点研发计划“植物源性食品中农药多残留检测技术创新研究”(2023JNZC175)

Review of Pre-treatment Methods for Pesticide Residue Detection in Fruits and Vegetables

OU Shuai(), MA Chengren, WANG Jingyuan, TIAN Xiuxiu, GAO Meng, GUO Xin   

  1. Liangshan County Inspection and Testing Center, Jining, Shandong 272600
  • Received:2024-06-25 Revised:2024-10-14 Published:2025-01-13 Online:2025-01-13

摘要:

为获得安全、可靠、省时、省力的农药残留检测前处理技术,本文综述了果蔬农药残留检测前处理技术的最新研究进展,重点讨论了固相萃取法(SPE)、基质分散固相萃取(MSPD)法、QuEChERS法、加速溶剂萃取法(ASE)、凝胶渗透色谱法(GPC)、分子印迹聚合物萃取(MIPs)法等前处理方法和纳米材料在果蔬农药残留检测中的应用,分析了各前处理方法在果蔬农药残留检测中的研究进展。综述发现,前处理技术仍是决定农药残留检测是否准确、高效的关键。同时对未来果蔬中前处理技术进行展望,旨在为果蔬中农药残留检验检测和食品安全监管提供理论参考。

关键词: 水果, 蔬菜, 农药残留, 前处理, 固相萃取, QuEChERS, 纳米材料, 基质分散固相萃取

Abstract:

In order to obtain a safe, reliable, time-saving and labor-saving pre-treatment technology for pesticide residue detection, this paper focused on the application of nanomaterials in the detection of pesticide residues in fruits and vegetables, discussing various pretreatment methods including solid phase extraction (SPE), matrix-dispersive solid phase extraction (MSPD), QuEChERS, accelerated solvent extraction (ASE), Gel permeation chromatography (GPC), and molecularly imprinted polymer Extraction (MIPs). The research progress in the detection of pesticide residues in fruits and vegetables was also analyzed. The review found that pre-treatment technology was still the key to determine whether the detection of pesticide residues was accurate and efficient. At the same time, the future pre-treatment technology of fruits and vegetables was prospected, aiming at providing theoretical reference for the inspection and detection of pesticide residues in fruits and vegetables and food safety supervision.

Key words: fruits, vegetables, pesticide residues, pre-treatment, solid phase extraction (SPE), QuEChERS, nanomaterials, matrix solid-phase disperse (MSPD)