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Chinese Agricultural Science Bulletin ›› 2014, Vol. 30 ›› Issue (6): 159-162.doi: 10.11924/j.issn.1000-6850.2013-0506

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Improvement in the H2SO4-H2O2 Digestion Method for Determining Plant Total Nitrogen

  

  • Received:2013-02-27 Revised:2013-04-19 Online:2014-02-25 Published:2014-02-25

Abstract: In order to determinate quickly and accurately, and improve the determining efficiency, H2SO4-H2O2 digestion method for determining plant total nitrogen was improved. H2O2 was added only once in digestion process. The coefficient of variation (CV) of the improved method was less than 5%. The recoveries were in the range of 95%-105%. The time of improved method was less 50-80 min than that of the original H2SO4-H2O2 digestion method. H2O2 consumption was saved 0.38 -0.68 mL per sample. Detection results were no significant difference between the two methods. Precision and accuracy met the requirement of detection analysis. The improved method was recommended as digestion method for rapid determining batch plant total nitrogen.