低氧贮存片烟解封后理化指标和质量变化研究

doi:10.11924/j.issn.1000-6850.casb2021-0418

中国农学通报 ›› 2022, Vol. 38 ›› Issue (4): 107-112.doi: 10.11924/j.issn.1000-6850.casb2021-0418

所属专题：生物技术；烟草种植与生产

• 食品·营养·检测·安全 • 上一篇下一篇

低氧贮存片烟解封后理化指标和质量变化研究

黄磊¹(), 李艺萌², 钟帅¹, 金保锋¹, 高晋军¹, 王晓园¹, 关罗浩¹, 王初亮¹, 黄妧婷¹, 李敏¹()

¹广东中烟工业有限责任公司原料供应中心,广州 510310
²华南理工大学食品科学与工程学院,广州,510640

收稿日期:2021-04-19 修回日期:2021-11-04 出版日期:2022-02-05 发布日期:2022-03-16
通讯作者: 李敏
作者简介:黄磊,男,1986年出生,湖南浏阳人,农艺师,研究方向为烟叶仓储醇化方面。通信地址：510310 广东中烟工业有限责任公司原料供应中心,E-mail： huanglei100200@qq.com。
基金资助:
广东中烟工业有限责任公司科技项目“不同氧气浓度氮气保护法片烟醇化周期研究”(粤烟工 [2020] 科字第004号)

Changes of Physical and Chemical Indexes of Tobacco Leaves Sealed with Hypoxia After Unsealing

HUNAG Lei¹(), LI Yimeng², ZHONG Shuai¹, JIN Baofeng¹, GAO Jinjun¹, WANG Xiaoyuan¹, GUAN Luohao¹, WANG Chuliang¹, HUANG Wanting¹, LI Min¹()

¹Raw Material Supply Center of Guangdong, China Tobacco Industry Co., Ltd., Guangzhou 510310
²South China University of Technology, School of Food Science and Engineering, Guangzhou 510640

Received:2021-04-19 Revised:2021-11-04 Online:2022-02-05 Published:2022-03-16
Contact: LI Min

摘要/Abstract

摘要：

烟叶经过复烤之后,通常还具有一些不能满足市场口味的品质,企业通常需将复烤后的烟叶进行一段时间的醇化处理,以协调烟叶内在化学成分,改善烟叶的品质。低氧贮存片烟是常用技术。笔者探究新烟入库即采用密封降氧贮存的复烤片烟使用时,解封后3个月内的碘值、pH、色差值、多酚氧化酶活性的变化,以及外观质量和感官质量的变化,分析解封后烟叶的性质变化趋势,旨在为合理安排密封降氧贮存的烟叶使用计划、精细化片烟仓储管理、保障烟叶使用品质提供参考。研究结果表明,烟叶解封后3个月内,烟叶碘值逐渐上升,pH在解封1个月内急速下降,2~3个月时逐渐维持稳定;色差值有所波动,多酚氧化酶活性逐渐增加。此外,持续低氧密封3个月的样品多酚氧化酶活性明显低于解封后自然放置3个月的样品,pH和碘值的变化幅度也明显小于解封后样品,其变化幅度接近于解封后自然放置1个月的样品。外观颜色评价表明,解封后自然放置3个月对湖南湘西B2F烟叶的色值影响最大,其次是香气和色度,对其均匀度、油分均基本无影响,对云南文山C3F颜色、均匀度、色度影响较大,对香气、油分均基本无影响,解封后自然放置3个月和持续低氧密封储存3个月的烟叶外观颜色评价得分几乎没有差别。本研究可较好评估低氧贮存的烟叶在解封后的性质变化,为低氧贮存的烟叶解封后的护理和应用提供借鉴。

关键词: 复烤烟叶, 密封降氧, 碘值, pH, 多酚氧化酶活性, 色差

Abstract:

After recuring, tobacco leaves usually have some qualities that cannot meet the taste requirement of the market, enterprises usually need to mellow the redried tobacco leaves for a period of time to coordinate the internal chemical components of tobacco leaves and improve the quality, and the technology of tobacco leaves sealed with hypoxia is often used. This study explored the changes of iodine value, pH, color difference value, polyphenol oxidase activity, appearance quality and sensory quality of tobacco leaves within 3 months after sealing, aiming to lay a foundation for the storage management, quality assurance and use of the tobacco leaves. The results showed that the iodine value of tobacco leaves gradually increased within 3 months after the unsealing, and the pH dropped rapidly within 1 month of unsealing and gradually remained stable after 2-3 months, the color difference values fluctuated, and the activity of polyphenol oxidase gradually increased. In addition, the polyphenol oxidase activity of the samples sealed for 3 months under hypoxia was significantly lower than those of the samples under natural storage for 3 months after unsealing, the pH value and polyphenol oxidase activity also had a smaller change range than that of the unsealing samples, and the change range was close to that under natural storage for 1 month after unsealing. Appearance color evaluation showed that natural storage for 3 months after unsealing had the greatest impact on the color value of Hunan Xiangxi B2F tobacco leaves, followed by the impact on aroma and chromaticity, but had no effect on the uniformity and oil content of the tobacco leaves. Besides, natural storage had a relatively great impact on the color, uniformity and chromaticity of Yunnan Wenshan C3F, and basically had no effect on aroma and oil content. And the two storage methods, natural storage for 3 months after unsealing and continuous sealed with hypoxia for 3 months, had almost no effect on the appearance color evaluation scores of tobacco leaves. The study evaluates the properties’ change of tobacco leaves stored in hypoxia after unsealing and lay a foundation for the processing and application of tobacco leaves stored in hypoxia after unsealing.

Key words: redried tobacco, sealed with hypoxia, iodine value, pH, polyphenol oxidase activity, color difference value

中图分类号:

TS41+1

黄磊, 李艺萌, 钟帅, 金保锋, 高晋军, 王晓园, 关罗浩, 王初亮, 黄妧婷, 李敏. 低氧贮存片烟解封后理化指标和质量变化研究[J]. 中国农学通报, 2022, 38(4): 107-112.

HUNAG Lei, LI Yimeng, ZHONG Shuai, JIN Baofeng, GAO Jinjun, WANG Xiaoyuan, GUAN Luohao, WANG Chuliang, HUANG Wanting, LI Min. Changes of Physical and Chemical Indexes of Tobacco Leaves Sealed with Hypoxia After Unsealing[J]. Chinese Agricultural Science Bulletin, 2022, 38(4): 107-112.

图/表 7

参考文献 26

[1]	管恩森, 孔芳芳, 王大海, 等. 烤烟自然醇化和人工醇化过程中感官质量的变化[J]. 中国烟草科学, 2020(2):54-58.
[2]	SUN J G, HE J W, WU F G, et al. Comparative analysis on chemical components and sensory quality of aging flue-cured tobacco from four main tobacco areas of China[J]. Agricultural sciences in China, 2011(8):1222-1231.
[3]	范坚强, 宋纪真, 赖成连, 等. 密封降氧抑制醇化过程中烟片颜色转深试验[J]. 烟草科技, 2005(12):23-26.
[4]	彭琛, 余其昌, 林锐峰, 等. 一种广东地区低氧贮存烟叶的夏秋季启用方法[P]. 中国专利,CN107495458A. 2017.
[5]	彭琛, 林锐峰, 任胜超, 等. 富氮控氧法对3种虫态烟草甲杀灭效果[J]. 中国农学通报, 2017, 33(31):122-126.
[6]	WU S, GUO Y, JOAN H I, et al. iTRAQ-based comparative proteomic analysis reveals high temperature accelerated leaf senescence of tobacco (Nicotiana tabacum L.) during flue-curing[J]. Genomics, 2020, 112(5).
[7]	MAHDAVI B, YAACOB W A, DIN L B. Phytochemical study of medicinal smokes from Etlingera brevilabrum leaves[J]. Journal of herbal medicine, 2018, 13:52-62. doi: 10.1016/j.hermed.2018.04.001 URL
[8]	WANG L, CHENG B, LI Z, et al. Intelligent tobacco flue-curing method based on leaf texture feature analysis[J]. Optik, 2017, 150:117-130. doi: 10.1016/j.ijleo.2017.09.088 URL
[9]	STANFILL S, CROUCHER R, GUPTA P, et al. Chemical characterization of smokeless tobacco products from South Asia: Nicotine, unprotonated nicotine, tobacco-specific N’-nitrosamines, and flavor compounds[J]. Food & chemical toxicology, 2018, 118:626-634.
[10]	李琳, 刘洋, 王豹祥, 等. 不同品种烟叶碘值吸光度值与评吸质量的相关性分析[J]. 江西农业学报, 2011, 23(10):94-96.
[11]	中国烟草标准化研究中心, 广东中烟工业公司, 郑州烟草研究院, 等. YC/T 222—2007,烟草及烟草制品 pH的测定[S]. 北京: 中国标准出版社, 2007:2-8.
[12]	陈飞程, 白金莹, 杨洋, 等. 不同成熟度烤烟色差参数与烘烤特性关系研究[J]. 江西农业学报, 2021, 33(2):78-82.
[13]	兰俊荣, 靖军领, 黄一兰, 等. 不同成熟度烟叶烘烤过程中多酚氧化酶活性变化[J]. 现代农业科技, 2010(23):54-55,57.
[14]	中国烟叶生产购销公司. GB 2635—1992,烤烟[S]. 北京:国家技术监督局, 1992:1-16.
[15]	司辉, 闫铁军, 张环宇, 等. 不同生态产区烤烟片烟化学成分在醇化中的变化规律研究[J]. 安徽农业科学, 2011, 39(22):13328-13333.
[16]	RAJAN A G, SIVASUBRAMANIAN M, GOWTHAMAN S, et al. Investigation of physical and chemical properties of tobacco seed oil fatty acid methyl ester for biodiesel production[J]. Materials today: proceedings, 2021(1).
[17]	谭小红. 复烤片烟自然醇化过程中品质变化研究[J]. 南方农机, 2016(47):77.
[18]	刘春奎, 贾琳, 王晓宾, 等. 广东烤烟总挥发碱、总挥发酸和pH的分析[J]. 南方农业学报, 2014, 45(9):1647-1651.
[19]	胡亚杰, 韦建玉, 宗钊辉, 等. 云南不同烟区片烟醇化过程色度及主要化学成分变化特征研究[J]. 中国农学通报, 2020, 36(22):143-153.
[20]	宗钊辉, 刘高, 韦建玉, 等. 基于色差值和色度值的醇化片烟褐变判定模型研究[J]. 南方农业学报, 2018, 49(10):2040-2046.
[21]	FERNANDES G M, SILVA W R, BARRETO D N, et al. Novel approaches for colorimetric measurements in analytical chemistry- A review[J]. Analytica chimica acta, 2020, 1135:187-203.
[22]	杨树勋. 烟草酶促棕色化反应机理及其调控研究进展[J]. 作物研究, 2019, 33(3):246-250.
[23]	KEPPLER J K, SCHWARZ K, GOOT A. Covalent modification of food proteins by plant-based ingredients (polyphenols and organosulphur compounds): A commonplace reaction with novel utilization potential[J]. Trends in food science & technology, 2020, 101:38-49.
[24]	宋怡, 夏建军, 丁中涛. 抗坏血酸对烟草中多酚类物质稳定性影响的研究[J]. 云南化工, 2008, 35(6):12-14.
[25]	CHEN J, LI Y, HE X, et al. Influences of different curing methods on chemical compositions in different types of tobaccos[J]. Industrial crops and products, 2021, 167(1):113534. doi: 10.1016/j.indcrop.2021.113534 URL
[26]	任胜超, 彭琛, 林锐峰, 等. 物理气调法片烟养护及醇化效果研究[J]. 中国农学通报, 2018, 34(8):95-103.

样品组	B2F		C3F
样品组	455 nm	483 nm	455 nm	483 nm
解封当时	0	0	0	0
解封1个月	-2.04	-5.56	2.38	1.32
解封2个月	7.69	7.29	3.33	0.92
解封3个月	9.35	8.74	9.13	11.61
低氧密封3个月	4.38	-0.66	3.23	6.07

样品组	B2F		C3F
样品组	455 nm	483 nm	455 nm	483 nm
解封当时	0	0	0	0
解封1个月	-2.04	-5.56	2.38	1.32
解封2个月	7.69	7.29	3.33	0.92
解封3个月	9.35	8.74	9.13	11.61
低氧密封3个月	4.38	-0.66	3.23	6.07

样品组	B2F	C3F
解封当时	0	0
解封1个月	1.65	1.57
解封2个月	1.99	2.05
解封3个月	1.78	2.05
低氧密封3个月	0.34	1.02

样品组	B2F	C3F
解封当时	0	0
解封1个月	1.65	1.57
解封2个月	1.99	2.05
解封3个月	1.78	2.05
低氧密封3个月	0.34	1.02

物料名称	解封时间	外观质量评价指标						综合得分
物料名称	解封时间	颜色	闻香	均匀度	身份	油分	色度	综合得分
2017/湖南湘西/B2F	当天	7.000	7.000	7.000	8.000	7.000	7.000	7.100
	1月后	6.000	6.500	7.000	8.000	7.000	6.500	6.675
	2月后	6.000	6.500	7.000	8.000	7.000	6.500	6.675
	3月后	5.500	6.500	7.000	8.000	7.000	6.500	6.550
	低氧密封3个月	5.750	6.500	7.000	8.000	7.000	6.500	6.613
2017/云南文山/C3F	当天	7.000	7.000	7.000	8.000	7.000	7.000	7.100
	1月后	6.500	7.000	6.500	8.000	7.000	6.500	6.825
	2月后	6.500	7.000	6.500	8.000	7.000	6.500	6.825
	3月后	6.500	7.000	6.500	8.000	7.000	6.500	6.825
	低氧密封3个月	6.500	7.000	6.500	8.000	7.000	6.500	6.825

低氧贮存片烟解封后理化指标和质量变化研究

Changes of Physical and Chemical Indexes of Tobacco Leaves Sealed with Hypoxia After Unsealing

RichHTML

PDF (PC)

可视化

摘要/Abstract

引用本文

使用本文

图/表 7

参考文献 26

相关文章 15

编辑推荐

Metrics

本文评价

关于本刊

作者中心

审者中心

在线期刊

联系我们

[1]	张云, 萨如拉, 包桂荣, 萨茹拉其其格, 邰继承, 李响. 秸秆降解菌系的筛选及其对酸碱度的响应[J]. 中国农学通报, 2022, 38(28): 21-27.
[2]	苏欣欣, 胡晓航, 马亚怀, 李彦丽. 滤泥施用量对不同品种甜菜产量及土壤中氮磷钾含量的影响[J]. 中国农学通报, 2022, 38(11): 38-45.
[3]	胡娟, 周道玮, 关胜超, 张丹. 覆沙对松嫩平原盐碱裸地的改良和利用效果研究[J]. 中国农学通报, 2021, 37(9): 85-94.
[4]	沐婵, 钱荣青, 杨绍聪, 姚照兵, 张钟, 李成春, 申文智, 费勇. 种植关键技术对‘灿烂’蓝莓叶片黄化症的矫治效果分析[J]. 中国农学通报, 2021, 37(7): 49-53.
[5]	刘天海, 苗人云, 陈春秀, 刘理旭, 周洁, 彭卫红, 黄忠乾, 谭昊. 石灰质量调查及添加量对糙皮侧耳熟料栽培的影响[J]. 中国农学通报, 2021, 37(6): 44-48.
[6]	刘霞, 张哲, 钱红洁, 张利杰, 杨艳丽. 致病疫霉木瓜蛋白酶亚家族基因C1A-PH-SCH1的克隆与表达分析[J]. 中国农学通报, 2021, 37(29): 13-19.
[7]	张琦林, 胡娟, 高英志, 周道玮. 松嫩平原沙丘-草甸复合生态系统土壤水分和盐碱时空变化特征[J]. 中国农学通报, 2021, 37(20): 49-58.
[8]	董环, 娄春荣, 张青, 韩瑛祚, 王辉. 调节草炭pH值对其有效养分和番茄、辣椒幼苗生长的影响[J]. 中国农学通报, 2020, 36(7): 55-62.
[9]	郑明, 白云岗, 张江辉, 丁邦新, 肖军. 基于主成分分析法的干旱区典型绿洲土壤盐分特征分析——以新疆第二师31团为例[J]. 中国农学通报, 2020, 36(27): 81-87.
[10]	刘绍波, 解鑫, 平文祥, 葛菁萍. 控制pH值和溶解氧对地衣芽孢杆菌HDYM-04分批发酵产β-甘露聚糖酶的影响[J]. 中国农学通报, 2020, 36(23): 26-30.
[11]	胡亚杰, 韦建玉, 宗钊辉, 陈泽鹏, 王军, 黄崇峻, 王行, 王维. 云南不同烟区片烟醇化过程色度及主要化学成分变化特征研究[J]. 中国农学通报, 2020, 36(22): 143-153.
[12]	贺爱国, 戴艳娇, 胡志鑫, 吴家梅, 陈锦. 不同pH条件下IBA和NAA对伴矿景天生根的影响研究[J]. 中国农学通报, 2020, 36(22): 49-54.
[13]	谭秋锦, 王文林, 陈海生, 郑树芳, 覃振师, 何铣扬, 黄锡云, 许鹏. 石漠化澳洲坚果园土壤养分及pH值空间异质性分析[J]. 中国农学通报, 2020, 36(2): 80-83.
[14]	谢红花,李超,钱晔,李文峰. 云南乌蒙山区土壤养分空间变异及海拔梯度分布规律[J]. 中国农学通报, 2019, 35(8): 52-59.
[15]	梁艳妮. 马齿苋总黄酮的超声波辅助提取工艺优化及其抗氧化、抗肿瘤活性研究[J]. 中国农学通报, 2019, 35(4): 130-135.