欢迎访问《中国农学通报》,

中国农学通报 ›› 2016, Vol. 32 ›› Issue (13): 172-176.doi: 10.11924/j.issn.1000-6850.casb15110080

所属专题: 油料作物 园艺

• 食品 营养 检测 安全 • 上一篇    下一篇

灭蝇胺在菜用大豆上的残留消解动态及安全性评价

陈丽萍   

  1. 漳州市农业检验监测中心
  • 收稿日期:2015-11-13 修回日期:2016-04-12 接受日期:2016-02-25 出版日期:2016-05-17 发布日期:2016-05-17
  • 通讯作者: 陈丽萍
  • 基金资助:
    漳州市科技计划项目“蔬菜农药残留监测及无公害生产技术研究”(Z03028)。

Residue Degradation Dynamics and Safety Assessment of Cyromazine on Vegetable Soybean

  • Received:2015-11-13 Revised:2016-04-12 Accepted:2016-02-25 Online:2016-05-17 Published:2016-05-17

摘要: 为了研究灭蝇胺在菜用大豆上的残留消解动态并对其进行安全评价,本研究采用液相色谱法及田间试验方法,研究了菜用大豆上灭蝇胺的残留量。试验表明:菜用大豆上灭蝇胺的原始残留量因不同施药方案有所差异,施用375 g a.i./hm2的原始残留量>施用187.5 g a.i./hm2的原始残留量;间隔7 天连续施用2 次的原始残留量>施用1 次;残留消解动态符合一级动力学方程,半衰期(T1/2)为5.6~6.1 天,T0.99为37.3~40.6 天;在最终残留试验区,灭蝇胺按常规施药量(187.5 g a.i./hm2)及施药方法,施药1 次与间隔7天连续施药2 次,在末次施药后15 天,最终残留量分别为0.132~0.194 mg/kg 和0.156~0.202 mg/kg,产品符合GB 2763—2014规定的豆类的MRL(0.5 mg/kg)要求。

关键词: 乌拉尔甘草, 乌拉尔甘草, 发根农杆菌, 毛状根, 诱导

Abstract: In order to study the residue degradation dynamics of cyromazine on vegetable soybean and conduct its safety assessment, liquid chromatography and field test were applied to analyze the residue amount. The results showed that the initial residue amounts of cyromazine on vegetable soybean were different in different pesticides application schemes. When the concentration was 375 g a.i./hm2, the initial residue amount was higher than that of 187.5 g a.i./hm2. When spraying cyromazine twice at 7 days interval, the initial residue amount was more than that of just one time spraying. The residue degradation dynamics of cyromazine on vegetable soybean was in conformity with the first-order kinetic equation, T1/2 was 5.6-6.1 d and T0.99 was 37.3-40.6 d. In the final residue test, cyromazine was sprayed for 187.5 g a.i./hm2 with the conventional method, spraying only one time and twice at 7 days interval, and after 15 days of the last application, the final residue amount of cyromazine was 0.132-0.194 mg/kg and 0.156-0.202 mg/kg, respectively, which could meet the requirement of MRL (0.5 mg/kg) in GB 2763—2014.